By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun
Read or Download 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium PDF
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Extra info for 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium
M − OH + OH − M − → − M − O − M − + H 2 O . (6) − M − OH + RO − M − → − M − O − M − + ROH . (7) The as synthesized aluminum-containing film, once pyrolysed, forms amorphous alumina. The pyrolysys is performed under a 1 bar argon atmosphere. The temperature is risen to 900°C and held for 4 hours. Then the samples are heat treated for 1 hour under a static 1 bar pressure, either at 26 12th INTERNATIONAL CERAMICS CONGRESS PART B 1200°C under an argon atmosphere to form α-Al2O3 or from 1200°C to 1600°C under a nitrogen atmosphere to form aluminum nitride.
During the experiment, a 2 ppm standard NO gas (balance N2) was mixed with air (1:1), and passed through the reactor (373 cm3 of internal volume) continuously throughout the reaction. 5 mm) of a glass holder plate and set in the bottle center of the reactor. The light was turned on after having reached the adsorption equilibrium with the flow of NO gas. The concentration of NO was determined using a NOx analyzer (Yanaco, ECL-88A). , Pyrex glass for λ>290nm, Kenko L41 Pro (W) for λ>400nm, and Fuji triacetyl cellulose filter for λ>510nm.
The commercial P25 TiO2 showed no absorption ability under visible light region, due to the large band gap energy of ca. 3 eV. The N doped TiO2 showed a two step absorption; the first absorption around 390 nm should be related to the band gap of TiO2, and the second absorption edge around 500 nm could be attributed to the newly formed N 1s orbit by the nitrogen doping in the molecular structure . By further co-doping Fe into the samples, absorption under visible light could be further enhanced.
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